Description of the workshop
In this workshop, the concepts of one dimensional NMR, with special emphasis on spectral patterns will be discussed. The nomenclatures of strong and weakly coupled spins systems, with examples, such as, AX, AB, A2, AMX, etc. will be discussed. analysis of spectra of 1H, 13C, 19F, 31P, 119Sn, and many other heteronuclei with numerous examples. The concept of polarization transfer techniques, viz., APT, INEPT, DEPT, will be discussed in detail. Conceptual understanding of two-dimensional spectra, the analysis of COSY, TOCSY, NOESY, HSQC, HMQC, HMBC, spectra will be provided. One dimensional versions of experiments, such as, TOCSY, NOESY, etc. and their utility will be introduced.
Mode of the Workshop: Online
Date & Timings:
23rd – 27th & 30th September, 2024 : 06:00 p.m. – 08:00 p.m.
28th & 29th September ,2024 : 10:00 a.m. – 12 Noon
Instructor Profile
Prof. N. Suryaprakash, served as the Chairman and Professor at the NMR Research Centre, Indian Institute of Science, Bangalore. His research work is focused on diverse wings of NMR spectroscopy, with a major focus on the manipulation of spin dynamics to design novel NMR techniques to combat inherent challenging problems of NMR spectroscopy, viz., to achieve sensitivity enhancement, higher resolution, discerning of degenerate transitions and facile extraction of spectral information. His designed single and multiple quantum methodologies significantly transformed chiral analysis of molecules in weakly aligned media using <sup>1</sup>H NMR. He has also discovered numerous water compatible weak chiral aligning media that circumvented many inherent limitations of enantiomeric differentiation. His seminal contributions have catapulted research in NMR spectroscopy, structural chemistry, chiral chemistry and in the field of weak molecular interactions. He is a world renowned leader in the field of NMR spectroscopy.
Intended Audience & Eligibility
Audience: MSc and PhD students, practicing NMR spectroscopists
Eligibility: MSc in Physics, Chemistry, Biology or Pharamaceutical Sciences.
Schedule
Day 1 – NMR Chemical Shifts, J couplings and Multiplicity Patterns
Day 2 – Analysis of 1D 1 H NMR Spectra
Day 3 – 13C NMR, DEPT
Day 4– Analysis of Spectra of Heteronuclei
Day 5 – 2D NMR, COSY and TOCSY and HSQC
Day 6 – HMBC, INADEQUATE, 2D NOESY
Day 7 – 1D NOE, 1D TOCSY and their utility
Day 8– Combined Utility of 1D and 2D Techniques
Fee Structure
Students: Rs 1180/- (1000+18%GST)
Faculty: Rs 1770/- (1500+18%GST)
Industry: Rs 2360/- (2000+18%GST)
Certification
Attendance and Final Assessment is the required criteria for the Certification
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